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This mini-review presents the existing solid-state magic-angle spinning NMR techniques aimed towards the efficient and accurate determination of inter-nuclear distances between a spin-1/2 and a 'quadrupolar' nucleus having a spin larger than one-half. A scheme for calculating nuclear magnetic resonance spin−spin coupling constants has been implemented in the Amsterdam density functional program system. The applicability of the frozen-core approximation is discussed, and an orbital analysis shows that the core orbitals of one of the nuclei can be significant. Results calculated with a modest Slater-type (exponential) basis set are. Martinez — who lives and works in Barcelona — is inspired by the great masters of photography that influenced him: Avedon, Beaton, Brandt, Walde Huth, and Edward Weston.
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Nuclear magnetic resonance (NMR) spectroscopy is one of the most powerful and widely used techniques in chemical research for investigating structures and dynamics of molecules. Advanced methods can even be utilized for structure determinations of biopolymers, for example proteins or nucleic acids. NMR is also used in medicine for magnetic resonance imaging (MRI). The method is based on.
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